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Spinodal Decomposition in a Model Colloid-Polymer Mixture in Microgravity

Last modified
Thursday, December 3, 2020 - 17:30
In Faculty Publications

Description

We study phase separation in a deeply quenched colloid-polymer mixture in microgravity on the International Space Station using small-angle light scattering and direct imaging. We observe a clear crossover from early-stage spinodal decomposition to late-stage, interfacial-tension-driven coarsening. Data acquired over 5 orders of magnitude in time show more than 3 orders of magnitude increase in domain size, following nearly the same evolution as that in binary liquid mixtures. The late-stage growth approaches the expected linear growth rate quite slowly.

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Article

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Limits to Gelation in Colloidal Aggregation

Last modified
Thursday, December 3, 2020 - 17:28
In Faculty Publications

Description

We show that the dynamics of large fractal colloid aggregates are well described by a combination of translational and rotational diffusion and internal elastic fluctuations, allowing both the aggregate size and internal elasticity to be determined by dynamic light scattering. The comparison of results obtained in microgravity and on Earth demonstrates that cluster growth is limited by gravity-induced restructuring. In the absence of gravity, thermal fluctuations ultimately inhibit fractal growth and set the fundamental limitation to the lowest volume fraction which will gel.

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Article

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Time-dependent strength of colloidal gels

Last modified
Wednesday, December 2, 2020 - 16:41
In Faculty Publications

Description

Colloidal silica gels are shown to stiffen with time, as demonstrated by both dynamic light scattering and bulk rheological measurements. Their elastic moduli increase as a power law with time, independent of particle volume fraction; however, static light scattering indicates that there are no large-scale structural changes. We propose that increases in local elasticity arising from bonding between neighboring colloidal particles can account for the strengthening of the network, while preserving network structure.

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Article

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Time-Dependent Strength of Colloidal Gels

Last modified
Wednesday, August 12, 2020 - 15:21
In Faculty Publications

Description

Colloidal silica gels are shown to stiffen with time, as demonstrated by both dynamic light scattering and bulk rheological measurements. Their elastic moduli increase as a power law with time, independent of particle volume fraction; however, static light scattering indicates that there are no large-scale structural changes. We propose that increases in local elasticity arising from bonding between neighboring colloidal particles can account for the strengthening of the network, while preserving network structure.

Type of Resource

Article

Rights Statements

In Copyright - Educational Use Permitted
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Spinodal Decomposition in a Model Colloid-Polymer Mixture in Microgravity

Last modified
Wednesday, August 12, 2020 - 15:09
In Faculty Publications

Description

We study phase separation in a deeply quenched colloid-polymer mixture in microgravity on the International Space Station using small-angle light scattering and direct imaging. We observe a clear crossover from early-stage spinodal decomposition to late-stage, interfacial-tension-driven coarsening. Data acquired over 5 orders of magnitude in time show more than 3 orders of magnitude increase in domain size, following nearly the same evolution as that in binary liquid mixtures. The late-stage growth approaches the expected linear growth rate quite slowly.

Type of Resource

Article

Rights Statements

In Copyright - Educational Use Permitted
Thumbnail for

Limits to Gelation in Colloidal Aggregation

Last modified
Wednesday, August 12, 2020 - 15:01
In Faculty Publications

Description

We show that the dynamics of large fractal colloid aggregates are well described by a combination of translational and rotational diffusion and internal elastic fluctuations, allowing both the aggregate size and internal elasticity to be determined by dynamic light scattering. The comparison of results obtained in microgravity and on Earth demonstrates that cluster growth is limited by gravity-induced restructuring. In the absence of gravity, thermal fluctuations ultimately inhibit fractal growth and set the fundamental limitation to the lowest volume fraction which will gel.

Type of Resource

Article

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In Copyright - Educational Use Permitted
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  • Article (6)

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  • Faculty Publications (6)

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Subject

  • Colloid-polymer mixtures in the presence of quenched disorder: a theoretical and computer simulation study. (1)
  • Colloidal aggregation affects the efficacy of anticancer drugs in cell culture (1)
  • Colloidal Gels with Extracellular Matrix Particles and Growth Factors for Bone Regeneration in Critical Size Rat Calvarial Defects. (1)
  • fractal colloid aggregates (1)
  • microgravity (1)

Authored on

  • (-) Show all (6)
  • March 2018 (6)

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